$x =~ s/([\x00-\x1F\ x7F-\xFF])/"\\'" .(unpack("H2",$1))/eg;
^
Assuming you're talking about Latin-1 characters (as the range up to just \xFF suggests), it should suffice to get rid of the indicated space...
my $x = "foo à, è, ì, ò, ù bar";
$x =~ s/([\x00-\x1F\x7F-\xFF])/"\\'" .(unpack("H2",$1))/eg;
print $x; # foo \'e0, \'e8, \'ec, \'f2, \'f9 bar
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